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I-laboratory pyrolysis yinkqubo ebalulekileyo yokufunda ukubola kwe-thermal yezinto phantsi kweemeko ezilawulwayo ngokungabikho kwe-oksijini. Obu buchule bufumene ukusetyenziswa ngokubanzi kuwo wonke amashishini afana nesayensi yezinto, uphando lokusingqongileyo, kunye nobunjineli bemichiza. Ukuqonda inkqubo yenyathelo ngenyathelo kunye nezixhobo ezisetyenziswayo - ezinje ngeigilasi ibhatyi pyrolysis reactor for labimifuniselo - ibalulekile ekufezekiseni iziphumo ezichanekileyo nezinokuphinda zenziwe kwakhona. Esi sikhokelo sintywila kwiziseko ze-labhoratri ye-pyrolysis, sigxininisa imiba ephambili yokuqinisekisa imifuniselo eyimpumelelo.

Yintoni iPyrolysis?
I-Pyrolysis yinkqubo yokuchithwa kwe-thermal eyenzeka xa izinto ziphantsi kobushushu obuphezulu kwindawo engenayo i-oxygen. Le nkqubo iqhekeza iikhompawundi ezintsonkothileyo zibe ziimolekyuli ezilula, ezivelisa iigesi, ulwelo, kunye neentsalela eziqinileyo njenge char. Kwiisetingi zaselabhoratri, i-pyrolysis ihlala isetyenziselwa ukufunda ukubunjwa kwezinto, i-kinetics yokusabela kovavanyo, kunye nokuphuhlisa izixhobo ezintsha okanye iinkqubo zekhemikhali.

Izixhobo ezingundoqo: I-Glass Jacketed Pyrolysis Reactor
Isixhobo se-pyrolysis esifakwe ngeglasi siqhele ukusetyenziswa kwi-lab-scale pyrolysis ngenxa yokuchaneka kwayo, ukungafihli, kunye nokukwazi ukulawula ubushushu. Uyilo lwejacket luvumela ukutshintshwa kobushushu obusebenzayo, ukuqinisekisa iimeko ezihambelanayo ze-thermal kuyo yonke inkqubo. Abaphandi banokubeka iliso kwiimpendulo ngexesha lokwenyani kwaye bahlengahlengise iiparamitha njengoko kufuneka, benze olu hlobo lwereactor lube lulungele iimeko ezilawulwayo zovavanyo.

Inkqubo yeNyathelo ngeNyathelo yePyrolysis yeLabhoratri
1. Ukulungiselela iSampuli
Khetha izinto eziza kuvavanywa, uqinisekise ukuba zomile kwaye ziphantsi zibe ngamaqhekeza afanayo xa kuyimfuneko.
Yenza umlinganiselo wesampulu ngokuchanekileyo ukugcina ukungaguquguquki kuyo yonke imifuniselo.
2. Ukulayisha iReactor
Beka isampuli kwigumbi lokusabela le-reactor.
Vala i-reactor ngokuqinileyo ukukhusela i-oksijini ekungeneni ngexesha lenkqubo.
3. Ukumisela iiParamitha zoMfuniselo
Seta uluhlu olufunekayo lobushushu, phakathi kwe-300 ° C kunye ne-900 ° C, ngokuxhomekeke kwizinto kunye neenjongo zovavanyo.
Lungisa umlinganiselo wokufudumeza ukulawula isantya sokubola kwe-thermal.
4. Ukucoca igesi engasebenziyo
Yazisa igesi engasebenziyo, efana nenitrogen okanye iargon, ukukhupha nayiphi na ioksijini eshiyekileyo.
Gcina ukuhamba okuzinzile kwegesi engasebenziyo kulo lonke ulingo ukuze uqinisekise indawo engenawo umoya-mpilo.
5. Isigaba sokufudumeza
Kancinci ukufudumeza i-reactor ngokweprofayili yobushushu obusetwe kwangaphambili.
Ukubeka iliso kwiqondo lokushisa ngokusondeleyo, njengoko izinga lokubola lingahluka kunye nobushushu.
6. Ukuqokelelwa kweMveliso
Njengoko i-pyrolysis isenzeka, qokelela igesi, ulwelo, kunye neemveliso eziqinileyo ngokusebenzisa iindawo ezifanelekileyo.
Sebenzisa iisistim zokujiya okanye zokuhluza ukwahlula nokubamba isigaba ngasinye ukuze kuhlalutywe ngakumbi.
7. Ukupholisa nokuhlalutya
Emva kokufikelela kwiqondo lobushushu ekujoliswe kulo kunye nokubamba ixesha elifunekayo lokusabela, zipholisa ngokuthe chu i-reactor ibuyele kwiqondo lobushushu begumbi.
Hlalutya iimveliso eziqokelelweyo usebenzisa ubuchule obufana nechromatography yegesi, i-mass spectrometry, okanye uhlalutyo lwe-thermal gravimetric.

Iingqwalasela eziphambili zePyrolysis eyimpumelelo
• Ulawulo lobushushu: Ulawulo oluchanekileyo lwamazinga okufudumeza kunye namaqondo obushushu ekujoliswe kuwo lubalulekile ekuveliseni kwakhona kunye nokuchaneka.
• I-Atmosphere ye-Inert: Nakuphi na ubukho be-oksijini kunokukhokelela ekutshiseni kunokuba i-pyrolysis, iguqule kakhulu iziphumo.
• Ubungakanani beSampuli kunye noKufana: Ubungakanani besampulu ehambelanayo kunye nokuhanjiswa okufanayo ngaphakathi kwereactor kuphucula ukuthembeka kweziphumo zovavanyo.
• Imilinganiselo yoKhuseleko: Iinkqubo zobushushu obuphezulu zifuna imigaqo yokhuseleko efanelekileyo, kuquka izixhobo zokukhusela kunye nokungena komoya okufanelekileyo.

Ukusetyenziswa kwePyrolysis yeLabhoratri
I-laboratory pyrolysis inezicelo ezahlukeneyo kwiinkalo ezahlukeneyo, kubandakanya:
• Uphuhliso lweMathiriyeli: Ukuphanda uzinzo lwe-thermal kunye neendlela zokubola kwezinto ezintsha.
• Izifundo zokusiNgqongileyo: Ukuhlalutya uguqulo lwe-biomass kunye neenkqubo zokucocwa kwenkunkuma.
• UPhando lweMichiza: Uphononongo lweendlela zokusabela kunye nokuvelisa iikhemikhali ezixabisekileyo ezivela kwizinto ezintsonkothileyo.

Ukuqukumbela
Ukufumana ubugcisa be-labhoratri ye-pyrolysis kufuna ukuqonda okunzulu kwenkqubo, ukuphathwa ngokufanelekileyo kwezixhobo ezifana neglasi efakwe i-pyrolysis reactor yovavanyo lwaselabhu, kunye nolawulo olucokisekileyo kwiiparamitha zovavanyo. Xa ziqhutywa ngokuchanekileyo, iimfuniselo zepyrolysis zibonelela ngemibono exabisekileyo ekuziphatheni kwezinto eziphathekayo kwaye zivule umnyango kwizinto ezintsha ezifunyenweyo kwiikhemikhali kunye nesayensi yezinto eziphathekayo.
Ngokulandela ezi zikhokelo, abaphandi banokwandisa ukuseta kwabo kwe-pyrolysis, baqinisekise iziphumo ezichanekileyo nezinokuphinda zenziwe kwakhona kulo lonke uvavanyo.

Ukufumana ulwazi oluthe kratya kunye neengcebiso zeengcali, ndwendwela iwebhusayithi yethu kuhttps://www.greendistillation.com/ukufunda ngakumbi malunga neemveliso kunye nezisombululo zethu.